| Case Studies
TRACERCO Diagnostics™ Leak Study
On Line detection of leaks for better shut down scheduling
Inter-stream leakage is a commonly occurring problem on
all types of process plant. A typical situation is where
water contamination of the liquid product from a distillation
unit may originate either from a leakage in the reboiler
or from a water leakage in one of the product condensers.
The problem facing the plant manager is to identify the
leak and to effect repairs in such a manner that shutdown-time
is minimized.

One obvious approach is to shut down the unit and subject
each of the suspect vessels to appropriate hydraulic or
pneumatic tests – a time consuming and expensive procedure.
Worse still, there is a possibility that the water contamination
does not originate from a leak at all, but from some upstream
process problem.
The TRACERCO Diagnostics™ Leak Study can provide
a way out of this dilemma and can assist the manager to
‘get it right first time’.
The TRACERCO Diagnostics™ Leak Study technique
involves testing the vessels online;
a) The reboiler is tested by injecting a gaseous tracer
radioisotope into the reboiler steam supply and sampling
the vapour from the return-line to the column. Any steam
leak will be revealed by the presence of tracer in the samples
and the size of the leak can be calculated from the measured
concentration.
b) Water leakage in the product condensers may be investigated
by injecting an aqueous tracer into the cooling water, sampling
and assaying the condensed product.

If a leak is identified by these procedures, the manager
can ensure that, at the shutdown, maintenance effort if
directed immediately towards the relevant vessel. If no
leak is identified, then immediate attention needs to be
given to identifying alternative sources of water contamination.
In either case, there are significant savings of shutdown
time and of maintenance effort.
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